Evaluating the Impact of Dispersants and Fluid Loss Additives on Cement Slurry Thickening Time: Experimental Design and Statistical Modeling
Keywords:
Cement, Slurry, modelling. Fuid, Loss, Dispersants.Abstract
Optimising cement slurry properties is critical for successful zonal isolation and preventing wellbore failures in oil and gas operations. This research investigated the effects of dispersant (0.1-1.0% BWOC) and fluid loss additive (0.1-0.35 gal/sk) concentrations on thickening time and free fluid formation of Class G cement slurry using a 3² factorial design. Thickening time was measured with an atmospheric consistometer; free fluid via HTHP filter press. Analysis included ANOVA and multiple regression modeling. Key findings Dispersant strongly influences thickening time (R² = 0.981, RMSE = 8.731 min). Fluid loss additive controls filtration and moderately affects thickening time. Significant dispersant-fluid loss additive interaction (p = 0.040) indicates synergistic effects. Models enable predictive optimization of cement slurry properties
References
Abbas, G., Irawan, S., Memon, K. R., & Khan, M. A. (2020). Hydroxy propyl methyl cellulose as free water and settling control agent in oil well cement slurry. Journal of Petroleum Exploration and Production Technology, 10(2), 319-325.
Ahmed, A., Mahmoud, A. A., Elkatatny, S., & Al-Majed, A. (2020). Improving Saudi class G oil-well cement properties using the tire wastes material. ACS Omega, 5(44), 27685-27691.
Bishop, M., & Barron, A. R. (2006). Cement hydration inhibition with sucrose, tartaric acids and lignosulfonates: Analytical and spectroscopic study. Industrial & Engineering Chemistry Research, 45(21), 7042-7049.
Cao, L., Guo, J., Tian, J., Xu, Y., Hu, M., Guo, C., & Fan, J. (2018). Synthesis, characterization and working mechanism of a novel sustained-release-type fluid loss additive for seawater cement slurry. Journal of Colloid and Interface Science, 524, 434-444.
Feng, J., Zhang, J., Feng, Q., & Li, S. (2023). Preparation and characterization of polymer retarder for plugging cement slurry. Journal of Dispersion Science and Technology, 44(12), 2239-2246.
Guo, S., Bu, Y., & Lu, Y. (2019). Addition of tartaric acid to prevent delayed setting of oil-well cement containing retarder at high temperatures. Journal of Petroleum Science and Engineering, 3(4), 1-8.
Hou, W., & Bao, J. (2019). Evaluation of cement retarding performance of cellulosic sugar acids. Construction and Building Materials, 202, 522-527.
Khalid, N. H. A., Hussin, M. W., Ismail, M., & Al-Majed, A. (2015). Evaluation of effectiveness of methyl methacrylate as retarder additive in polymer concrete. Construction and Building Materials, 93, 449-456.
Liu, C. J., Huang, B. Z., Xu, T. T., & Liu, J. (2015). Oil and gas well cementing theory and applications. Petroleum Industry Press, 84-90.
Magarini, P., Lanzetta, C., & Galletta, A. (1999). Drilling design. Manual Eni-Agip, Division, 97-107.
Michaux, M., & Nelson, E. B. (1990). Chemistry and characterization of Portland cement in well cementing. Nelson Elsevier Science Publishers Amsterdam, 8-25.
Moreira, P. H., Freitas, J. C., Braga, R. M., & Araújo, R. M. (2018). Production of carboxymethyl lignin from sugar cane bagasse: A cement retarder additive for oilwell application. Industrial Crops and Products, 116, 144-149.
Nelson, E. B., & Baret, J. F. (1990). Cement additives and mechanism of action in well cementing. Nelson Elsevier Science Publishers Amsterdam, 3-37.
Otunyo, W. A., & Koate, I. (2015). Sugar cane juice as a retarding admixture in concrete production. Global Journal of Engineering Research, 14, 17-23.
Roshan, H., & Asef, M. R. (2010). Characteristics of oil well cement slurry using CMC. Journal of Society of Petroleum Engineers Drilling and Completion, 25(3), 328-335.
Salam, K. K., Arinkoola, A. O., Ajagbe, B., & Oke, E. O. (2013). Evaluation of thickening time of oil field class G cement slurry at high temperature and pressure using experimental design. International Journal of Engineering Sciences, 2(11), 361-367.







